The union was not a success

The union was not a success, however.[26] Following a military overthrow led by Abd al-Karim al-Nahlawi on 28 September 1961, Syria seceded, reestablishing itself as the Syrian Arab Republic. Instability characterized the next 18 months, with various overthorws culminating on 8 March 1963, in the installation by leftist Syrian Army officers of the National Council of the Revolutionary Command (NCRC), a group of military and civilian officials who assumed control of all executive and legislative authority. The takeover was engineered by members of the Arab Socialist Resurrection Party (Baath Party), which had been active in Syria and other Arab countries since the late 1940s. The new cabinet was dominated by Baath members.[25][26]

The Baath takeover in Syria followed a Baath overthrow in Iraq the previous month. The new Syrian Government explored the possibility of federation with Egypt and with Baath-controlled Iraq.[26] An agreement was concluded in Cairo on 17 April 1963, for a referendum on unity to be held in September 1963. However, serious disagreements among the parties soon developed, and the tripartite federation failed to materialize. Thereafter, the Baath government in Syria and Iraq began to work for bilateral unity. These plans floundered in November 1963, when the Baath government in Iraq was overthrown.

In May 1964, President Amin Hafiz of the NCRC promulgated a provisional constitution providing for a National Council of the Revolution (NCR), an appointed legislature composed of representatives of mass organizations—labour, peasant, and professional unions—a presidential council, in which executive power was vested, and a cabinet. On 23 February 1966, a group of army officers carried out a successful, intra-party overthrow, imprisoned President Hafiz, dissolved the cabinet and the NCR, abrogated the provisional constitution, and designated a regionalist, civilian Baath government on 1 March.[26] The leaders of the overthrow described it as a "rectification" of Baath Party principles.

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